High Temperature oxidation evaluation using crystal microbalance - IFPEN - IFP Energies nouvelles Accéder directement au contenu
Article Dans Une Revue Corrosion Engineering, Science and Technology Année : 2020

High Temperature oxidation evaluation using crystal microbalance

Résumé

High-temperature oxidising environments are frequently encountered but the limited number of in situ techniques that can be implemented has hindered the monitoring possibilities and a better comprehension of the oxidation phenomenon. In this paper the high temperature oxidation behaviours of three alloys (AISI 316L, AISI 310 and HAYNES ® HR-120 ®) were studied by using crystal microbalances and surface characterizations. For the microbalance experiments two types of crystal were tested: quartz or gallium orthophosphate crystals. First the behaviour of thin sputtered deposited alloys on quartz slides was studied at 400 and 700°C under air oxidising conditions and compared to bulk samples. Kinetics measurements were performed on the three alloy films deposited on the resonators at 400 or 700°C under air. After the calibration of quartz and gallium orthophosphate crystals, it was possible to measure very small mass variations associated with thin oxide formation between 5 and 180 nm of thickness. The crystal microbalance technique gives very promising perspectives in understanding the high-temperature corrosion and scaling mechanisms and also for in situ monitoring.

Domaines

Matériaux
Fichier principal
Vignette du fichier
CST3722.pdf (1.12 Mo) Télécharger le fichier
Origine : Fichiers produits par l'(les) auteur(s)
Loading...

Dates et versions

hal-02539436 , version 1 (10-04-2020)

Identifiants

Citer

Michael Nicoli, François Grosjean, Rémy Mingant, Jean Kittel, Monica Trueba, et al.. High Temperature oxidation evaluation using crystal microbalance. Corrosion Engineering, Science and Technology, 2020, 55 (5), pp.365-371. ⟨10.1080/1478422X.2020.1732122⟩. ⟨hal-02539436⟩
97 Consultations
118 Téléchargements

Altmetric

Partager

Gmail Facebook X LinkedIn More